Crystallography Open Database

Information card for entry 7703342

Preview

Coordinates	7703342.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C46.5 H67 N4 O Si2 Y
Calculated formula	C46.5 H67 N4 O Si2 Y
Title of publication	Bis(alkyl) scandium and yttrium complexes coordinated by an amidopyridinate ligand: synthesis, characterization and catalytic performance in isoprene polymerization, hydroelementation and carbon dioxide hydrosilylation.
Authors of publication	Gurina, G. A.; Kissel, A. A.; Lyubov, D. M.; Luconi, L.; Rossin, A.; Tuci, G.; Cherkasov, A. V.; Lyssenko, K. A.; Shavyrin, A. S.; Ob'edkov, A. M.; Giambastiani, G.; Trifonov, A. A.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	3
Pages of publication	638 - 650
a	22.286 ± 0.001 Å
b	15.6506 ± 0.0007 Å
c	26.8173 ± 0.0012 Å
α	90°
β	90.918 ± 0.001°
γ	90°
Cell volume	9352.4 ± 0.7 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1029
Residual factor for significantly intense reflections	0.059
Weighted residual factors for significantly intense reflections	0.12
Weighted residual factors for all reflections included in the refinement	0.1383
Goodness-of-fit parameter for all reflections included in the refinement	1.056
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
247075 (current)	2020-01-22	cif/ Adding structures of 7703341, 7703342, 7703343 via cif-deposit CGI script.	7703342.cif