Crystallography Open Database

Information card for entry 7703990

Preview

Coordinates	7703990.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H96 K2 N10 O12 Zn2
Calculated formula	C48 H96 K2 N10 O12 Zn2
Title of publication	Intermediates and products of the reaction of Zn(ii) organyls with tetrel element Zintl ions: cluster extension versus complexation.
Authors of publication	Wallach, C.; Mayer, K.; Henneberger, T.; Klein, W.; Fässler, T F
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	19
Pages of publication	6191 - 6198
a	11.963 ± 0.005 Å
b	12.328 ± 0.005 Å
c	12.683 ± 0.006 Å
α	107.43 ± 0.04°
β	106.66 ± 0.04°
γ	104.16 ± 0.03°
Cell volume	1594 ± 1.5 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1097
Residual factor for significantly intense reflections	0.051
Weighted residual factors for significantly intense reflections	0.1003
Weighted residual factors for all reflections included in the refinement	0.1106
Goodness-of-fit parameter for all reflections included in the refinement	0.768
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
252774 (current)	2020-06-05	cif/ Updating files of 7703988, 7703989, 7703990, 7703991, 7703992, 7703993, 7703994, 7703995 Original log message: Adding full bibliography for 7703988--7703995.cif.	7703990.cif
250479	2020-04-08	cif/ Adding structures of 7703988, 7703989, 7703990, 7703991, 7703992, 7703993, 7703994, 7703995 via cif-deposit CGI script.	7703990.cif