Crystallography Open Database

Information card for entry 7703991

Preview

Coordinates	7703991.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H39 K0.84 O6 Rb0.16 Zn
Calculated formula	C30 H39 K0.843 O6 Rb0.157 Zn
Title of publication	Intermediates and products of the reaction of Zn(ii) organyls with tetrel element Zintl ions: cluster extension versus complexation.
Authors of publication	Wallach, C.; Mayer, K.; Henneberger, T.; Klein, W.; Fässler, T F
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	19
Pages of publication	6191 - 6198
a	21.842 ± 0.002 Å
b	7.2588 ± 0.0015 Å
c	18.322 ± 0.003 Å
α	90°
β	90°
γ	90°
Cell volume	2904.9 ± 0.8 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	6
Space group number	29
Hermann-Mauguin space group symbol	P c a 21
Hall space group symbol	P 2c -2ac
Residual factor for all reflections	0.1647
Residual factor for significantly intense reflections	0.054
Weighted residual factors for significantly intense reflections	0.0902
Weighted residual factors for all reflections included in the refinement	0.1059
Goodness-of-fit parameter for all reflections included in the refinement	0.655
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
252774 (current)	2020-06-05	cif/ Updating files of 7703988, 7703989, 7703990, 7703991, 7703992, 7703993, 7703994, 7703995 Original log message: Adding full bibliography for 7703988--7703995.cif.	7703991.cif
250479	2020-04-08	cif/ Adding structures of 7703988, 7703989, 7703990, 7703991, 7703992, 7703993, 7703994, 7703995 via cif-deposit CGI script.	7703991.cif