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Information card for entry 1545231
Preview
| Coordinates | 1545231.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C17 H30 N O3 Si |
|---|---|
| Calculated formula | C17 H31 N O3 Si |
| SMILES | [Si](OC(=C(C)\C=C)\N1[C@H](COC1=O)C(C)C)(C(C)(C)C)(C)C |
| Title of publication | Remote Asymmetric Induction Using Acetate-Type Vinylketene Silyl N,O-Acetals. |
| Authors of publication | Sagawa, Naoya; Sato, Haruka; Hosokawa, Seijiro |
| Journal of publication | Organic letters |
| Year of publication | 2017 |
| Journal volume | 19 |
| Journal issue | 1 |
| Pages of publication | 198 - 201 |
| a | 7.5929 ± 0.0003 Å |
| b | 11.2125 ± 0.0005 Å |
| c | 23.7488 ± 0.001 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 2021.86 ± 0.15 Å3 |
| Cell temperature | 273 K |
| Ambient diffraction temperature | 273 K |
| Number of distinct elements | 5 |
| Space group number | 19 |
| Hermann-Mauguin space group symbol | P 21 21 21 |
| Hall space group symbol | P 2ac 2ab |
| Residual factor for all reflections | 0.0535 |
| Residual factor for significantly intense reflections | 0.0476 |
| Weighted residual factors for significantly intense reflections | 0.1254 |
| Weighted residual factors for all reflections included in the refinement | 0.1285 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.208 |
| Diffraction radiation wavelength | 1.54187 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 191323 (current) | 2017-02-04 | cif/ Adding structures of 1545231 via cif-deposit CGI script. |
1545231.cif |
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Users of the data should acknowledge the original authors of the
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