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Information card for entry 1555325
Preview
| Coordinates | 1555325.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | 12mem_dimer |
|---|---|
| Formula | C17 H31 Si |
| Calculated formula | C17 H31 Si |
| Title of publication | Oxidative Dimerization of Silylallenes via Activation of the Allenic C(sp(2))-H Bond Catalyzed by Copper(I) Chloride and N-Hydroxyphthalimide. |
| Authors of publication | Sabbasani, Venkata R.; Lee, Daesung |
| Journal of publication | Organic letters |
| Year of publication | 2015 |
| Journal volume | 17 |
| Journal issue | 19 |
| Pages of publication | 4878 - 4881 |
| a | 6.5951 ± 0.0014 Å |
| b | 11.238 ± 0.003 Å |
| c | 12.03 ± 0.003 Å |
| α | 105.996 ± 0.006° |
| β | 93.545 ± 0.006° |
| γ | 94.888 ± 0.006° |
| Cell volume | 850.6 ± 0.4 Å3 |
| Cell temperature | 200 ± 2 K |
| Ambient diffraction temperature | 200 ± 2 K |
| Number of distinct elements | 3 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0807 |
| Residual factor for significantly intense reflections | 0.0526 |
| Weighted residual factors for significantly intense reflections | 0.1526 |
| Weighted residual factors for all reflections included in the refinement | 0.1784 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.154 |
| Diffraction radiation wavelength | 0.71073 Å |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 238484 (current) | 2019-11-24 | cif/ Adding structures of 1555325 via cif-deposit CGI script. |
1555325.cif |
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Users of the data should acknowledge the original authors of the
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