Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 1555326
Preview
| Coordinates | 1555326.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C13 H23 Si |
|---|---|
| Calculated formula | C13 H23 Si |
| Title of publication | Oxidative Dimerization of Silylallenes via Activation of the Allenic C(sp(2))-H Bond Catalyzed by Copper(I) Chloride and N-Hydroxyphthalimide. |
| Authors of publication | Sabbasani, Venkata R.; Lee, Daesung |
| Journal of publication | Organic letters |
| Year of publication | 2015 |
| Journal volume | 17 |
| Journal issue | 19 |
| Pages of publication | 4878 - 4881 |
| a | 6.2702 ± 0.0009 Å |
| b | 10.955 ± 0.0019 Å |
| c | 11.088 ± 0.0019 Å |
| α | 75.965 ± 0.005° |
| β | 74.11 ± 0.005° |
| γ | 74.699 ± 0.005° |
| Cell volume | 694.6 ± 0.2 Å3 |
| Cell temperature | 200 ± 2 K |
| Ambient diffraction temperature | 200 ± 2 K |
| Number of distinct elements | 3 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1155 |
| Residual factor for significantly intense reflections | 0.0964 |
| Weighted residual factors for significantly intense reflections | 0.3005 |
| Weighted residual factors for all reflections included in the refinement | 0.3182 |
| Goodness-of-fit parameter for all reflections included in the refinement | 2.442 |
| Diffraction radiation wavelength | 0.71073 Å |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 238486 (current) | 2019-11-24 | cif/ Adding structures of 1555326 via cif-deposit CGI script. |
1555326.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.