Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 1566524
Preview
| Coordinates | 1566524.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C74 H104 Ga2 N8 Sb2 |
|---|---|
| Calculated formula | C74 H104 Ga2 N8 Sb2 |
| Title of publication | Synthesis of Distibiranes and Azadistibiranes by Cycloaddition Reactions of Distibenes with Diazomethanes and Azides |
| Authors of publication | Weinert, Hanns Micha; Wölper, Christoph; Schulz, Stephan |
| Journal of publication | Chemical Science |
| Year of publication | 2022 |
| a | 10.4552 ± 0.0004 Å |
| b | 11.9732 ± 0.0004 Å |
| c | 14.9227 ± 0.0005 Å |
| α | 93.2189 ± 0.0014° |
| β | 97.3354 ± 0.0014° |
| γ | 107.995 ± 0.0014° |
| Cell volume | 1753.06 ± 0.11 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0219 |
| Residual factor for significantly intense reflections | 0.0191 |
| Weighted residual factors for significantly intense reflections | 0.0525 |
| Weighted residual factors for all reflections included in the refinement | 0.0543 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.079 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 273286 (current) | 2022-03-04 | cif/ Adding structures of 1566524, 1566525, 1566526, 1566527, 1566528, 1566529, 1566530, 1566531, 1566532, 1566533, 1566534, 1566535, 1566536 via cif-deposit CGI script. |
1566524.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.