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Information card for entry 1566525
Preview
| Coordinates | 1566525.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C66 H102 Ga2 N4 O2 Sb2 Si |
|---|---|
| Calculated formula | C66 H102 Ga2 N4 O2 Sb2 Si |
| Title of publication | Synthesis of Distibiranes and Azadistibiranes by Cycloaddition Reactions of Distibenes with Diazomethanes and Azides |
| Authors of publication | Weinert, Hanns Micha; Wölper, Christoph; Schulz, Stephan |
| Journal of publication | Chemical Science |
| Year of publication | 2022 |
| a | 59.557 ± 0.006 Å |
| b | 11.8135 ± 0.0012 Å |
| c | 21.011 ± 0.002 Å |
| α | 90° |
| β | 108.078 ± 0.003° |
| γ | 90° |
| Cell volume | 14053 ± 2 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.0995 |
| Residual factor for significantly intense reflections | 0.0755 |
| Weighted residual factors for significantly intense reflections | 0.1676 |
| Weighted residual factors for all reflections included in the refinement | 0.1812 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.125 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 273286 (current) | 2022-03-04 | cif/ Adding structures of 1566524, 1566525, 1566526, 1566527, 1566528, 1566529, 1566530, 1566531, 1566532, 1566533, 1566534, 1566535, 1566536 via cif-deposit CGI script. |
1566525.cif |
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Users of the data should acknowledge the original authors of the
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