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Information card for entry 1567695
Preview
Coordinates | 1567695.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C32 H30 O2 |
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Calculated formula | C32 H30 O2 |
Title of publication | [2 + 2] Cycloaddition of phosphaalkenes as a key step for the reductive coupling of diaryl ketones to tetraaryl olefins |
Authors of publication | Arkhypchuk, Anna I.; D'Imperio, Nicolas; Wells, Jordann A. L.; Ott, Sascha |
Journal of publication | Chemical Science |
Year of publication | 2022 |
Journal volume | 13 |
Journal issue | 41 |
Pages of publication | 12239 - 12244 |
a | 9.5099 ± 0.0004 Å |
b | 9.8152 ± 0.0004 Å |
c | 13.7004 ± 0.0005 Å |
α | 90° |
β | 105.846 ± 0.001° |
γ | 90° |
Cell volume | 1230.22 ± 0.09 Å3 |
Cell temperature | 170 K |
Ambient diffraction temperature | 170 K |
Number of distinct elements | 3 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0586 |
Residual factor for significantly intense reflections | 0.0438 |
Weighted residual factors for significantly intense reflections | 0.0939 |
Weighted residual factors for all reflections included in the refinement | 0.1015 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.066 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
278968 (current) | 2022-11-07 | cif/ Updating files of 1567695, 1567696, 1567697, 1567698, 1567699 Original log message: Adding full bibliography for 1567695--1567699.cif. |
1567695.cif |
278267 | 2022-09-30 | cif/ Adding structures of 1567695, 1567696, 1567697, 1567698, 1567699 via cif-deposit CGI script. |
1567695.cif |
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Users of the data should acknowledge the original authors of the
structural data.