Crystallography Open Database

Information card for entry 1569253

Preview

Coordinates	1569253.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C21 H33 I Mo N2 O3 P2
Calculated formula	C21 H33 I Mo N2 O3 P2
Title of publication	A synthetic cycle for iminophosphorane synthesis involving direct intermolecular NP bond formation on N<sub>2</sub>-derived molybdenum nitride.
Authors of publication	Jin, Li; Zhang, Guoqiang; Yang, Xiaoqin; Song, Jinyi; Wang, Jin; Liao, Qian
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2023
Journal volume	59
Journal issue	51
Pages of publication	7955 - 7958
a	25.9591 ± 0.0003 Å
b	13.17384 ± 0.00015 Å
c	14.86566 ± 0.00017 Å
α	90°
β	90°
γ	90°
Cell volume	5083.77 ± 0.1 Å³
Cell temperature	170 ± 2 K
Ambient diffraction temperature	170 ± 2 K
Number of distinct elements	7
Space group number	43
Hermann-Mauguin space group symbol	F d d 2
Hall space group symbol	F 2 -2d
Residual factor for all reflections	0.0378
Residual factor for significantly intense reflections	0.0374
Weighted residual factors for significantly intense reflections	0.1007
Weighted residual factors for all reflections included in the refinement	0.101
Goodness-of-fit parameter for all reflections included in the refinement	1.087
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
284833 (current)	2023-07-05	cif/ Updating files of 1569251, 1569252, 1569253, 1569254, 1569255, 1569256 Original log message: Adding full bibliography for 1569251--1569256.cif.	1569253.cif
284101	2023-06-01	cif/ Adding structures of 1569251, 1569252, 1569253, 1569254, 1569255, 1569256 via cif-deposit CGI script.	1569253.cif