Crystallography Open Database

Information card for entry 1569254

Preview

Coordinates	1569254.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H69 I3 Mo N2 Na O7 P2
Calculated formula	C36 H69 I3 Mo N2 Na O7 P2
Title of publication	A synthetic cycle for iminophosphorane synthesis involving direct intermolecular NP bond formation on N<sub>2</sub>-derived molybdenum nitride.
Authors of publication	Jin, Li; Zhang, Guoqiang; Yang, Xiaoqin; Song, Jinyi; Wang, Jin; Liao, Qian
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2023
Journal volume	59
Journal issue	51
Pages of publication	7955 - 7958
a	11.1871 ± 0.0003 Å
b	18.9167 ± 0.0005 Å
c	22.6936 ± 0.0006 Å
α	90°
β	90°
γ	90°
Cell volume	4802.5 ± 0.2 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	8
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.023
Residual factor for significantly intense reflections	0.022
Weighted residual factors for significantly intense reflections	0.0557
Weighted residual factors for all reflections included in the refinement	0.0561
Goodness-of-fit parameter for all reflections included in the refinement	1.032
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
284833 (current)	2023-07-05	cif/ Updating files of 1569251, 1569252, 1569253, 1569254, 1569255, 1569256 Original log message: Adding full bibliography for 1569251--1569256.cif.	1569254.cif
284101	2023-06-01	cif/ Adding structures of 1569251, 1569252, 1569253, 1569254, 1569255, 1569256 via cif-deposit CGI script.	1569254.cif