Crystallography Open Database

Information card for entry 1570317

Preview

Coordinates	1570317.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C53 H77 F3 Ge O7 P2 S
Calculated formula	C53 H77 F3 Ge O7 P2 S
Title of publication	Intramolecular donor-stabilized tetra-coordinated germanium(iv) di-cations and their Lewis acidic properties.
Authors of publication	Peddi, Balakrishna; Khan, Souvik; Gonnade, Rajesh G.; Yildiz, Cem B.; Majumdar, Moumita
Journal of publication	Chemical science
Year of publication	2023
Journal volume	14
Journal issue	47
Pages of publication	13755 - 13764
a	13.481 ± 0.003 Å
b	9.414 ± 0.002 Å
c	21.087 ± 0.004 Å
α	90°
β	96.178 ± 0.007°
γ	90°
Cell volume	2660.6 ± 1 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	7
Hermann-Mauguin space group symbol	P 1 n 1
Hall space group symbol	P -2yac
Residual factor for all reflections	0.1244
Residual factor for significantly intense reflections	0.0561
Weighted residual factors for significantly intense reflections	0.1493
Weighted residual factors for all reflections included in the refinement	0.1805
Goodness-of-fit parameter for all reflections included in the refinement	1.052
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
288746 (current)	2024-01-06	cif/ Updating files of 1570312, 1570313, 1570314, 1570315, 1570316, 1570317, 1570318, 1570319, 1570320, 1570321, 1570322, 1570323, 1570324, 1570325, 1570326, 1570327 Original log message: Adding full bibliography for 1570312--1570327.cif.	1570317.cif
287656	2023-11-17	cif/ Adding structures of 1570312, 1570313, 1570314, 1570315, 1570316, 1570317, 1570318, 1570319, 1570320, 1570321, 1570322, 1570323, 1570324, 1570325, 1570326, 1570327 via cif-deposit CGI script.	1570317.cif