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Information card for entry 2018926
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| Coordinates | 2018926.cif |
|---|---|
| Structure factors | 2018926.hkl |
| Original IUCr paper | HTML |
| Chemical name | Tetrakis[μ~3~-(pyridin-2-yl)methanolato]-<i>tetrahedro</i>-tetrakis[chloridolead(II)] |
|---|---|
| Formula | C24 H24 Cl4 N4 O4 Pb4 |
| Calculated formula | C24 H24 Cl4 N4 O4 Pb4 |
| SMILES | [O]12([Pb]3(Cl)[O]4(Cc5ccccn5)[Pb]1(Cl)[O]1(Cc5ccccn5)[Pb]2([O]3(Cc2ccccn2)[Pb]41Cl)Cl)Cc1ccccn1 |
| Title of publication | Two novel lead(II) complexes of 2-(hydroxymethyl)pyridine: a threefold diamondoid supramolecular network based on Pb~4~O~4~ cores and a two-dimensional (4,4) network based on Pb~2~O~2~ units |
| Authors of publication | Liu, Ting; Pan, Yu-Peng; Wang, Suna; Dou, Jian-Min |
| Journal of publication | Acta Crystallographica Section C |
| Year of publication | 2013 |
| Journal volume | 69 |
| Journal issue | 4 |
| Pages of publication | 394 - 399 |
| a | 15.373 ± 0.003 Å |
| b | 15.373 ± 0.003 Å |
| c | 13.287 ± 0.002 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 3140.1 ± 1 Å3 |
| Cell temperature | 298 ± 2 K |
| Ambient diffraction temperature | 298 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 88 |
| Hermann-Mauguin space group symbol | I 41/a :2 |
| Hall space group symbol | -I 4ad |
| Residual factor for all reflections | 0.0375 |
| Residual factor for significantly intense reflections | 0.026 |
| Weighted residual factors for significantly intense reflections | 0.0572 |
| Weighted residual factors for all reflections included in the refinement | 0.0609 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.14 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 180858 (current) | 2016-04-02 | cif/2/01/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/01/89. |
2018926.cif 2018926.hkl |
| 176760 | 2016-02-20 | cif/2/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/01. |
2018926.cif 2018926.hkl |
| 88055 | 2013-08-28 | cod/cif/ (saulius@koala.ibt.lt) Adding the _cod_database_fobs_code links for those COD CIFs that have their Fobs deposited recently. |
2018926.cif 2018926.hkl |
| 88054 | 2013-08-28 | cod/hkl/ (saulius@koala.ibt.lt) Adding Fobs files for the recently deposited IUCr coordinate data. |
2018926.cif 2018926.hkl |
| 85444 | 2013-05-07 | cif/ Adding structures of 2018926, 2018927 via cif-deposit CGI script. |
2018926.cif |
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Users of the data should acknowledge the original authors of the
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