Crystallography Open Database

Information card for entry 2018927

2018926 << 2018927 >> 2018928

Preview

Coordinates	2018927.cif
Original IUCr paper	HTML

Structure parameters

Chemical name	Poly[(μ~2~-nitrato)[μ~2~-(pyridin-2-yl)methanolato]lead(II)]
Formula	C6 H6 N2 O4 Pb
Calculated formula	C6 H6 N2 O4 Pb
SMILES	c1cccc2C[O]3[Pb]([n]12)[O]1Cc2cccc[n]2[Pb]31.N(=O)(=O)[O-].N(=O)(=O)[O-]
Title of publication	Two novel lead(II) complexes of 2-(hydroxymethyl)pyridine: a threefold diamondoid supramolecular network based on Pb~4~O~4~ cores and a two-dimensional (4,4) network based on Pb~2~O~2~ units
Authors of publication	Liu, Ting; Pan, Yu-Peng; Wang, Suna; Dou, Jian-Min
Journal of publication	Acta Crystallographica Section C
Year of publication	2013
Journal volume	69
Journal issue	4
Pages of publication	394 - 399
a	10.0543 ± 0.0015 Å
b	10.3292 ± 0.0016 Å
c	8.3716 ± 0.0009 Å
α	90°
β	91.388 ± 0.002°
γ	90°
Cell volume	869.2 ± 0.2 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0463
Residual factor for significantly intense reflections	0.0366
Weighted residual factors for significantly intense reflections	0.0856
Weighted residual factors for all reflections included in the refinement	0.09
Goodness-of-fit parameter for all reflections included in the refinement	1.051
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176760 (current)	2016-02-20	cif/2/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/01.	2018927.cif
85444	2013-05-07	cif/ Adding structures of 2018926, 2018927 via cif-deposit CGI script.	2018927.cif