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Information card for entry 2022926
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| Coordinates | 2022926.cif |
|---|---|
| Structure factors | 2022926.hkl |
| Original IUCr paper | HTML |
| Chemical name | Diaquabis(<i>o</i>-phenylenediamine-κ^2^<i>N</i>,<i>N</i>')nickel(II) naphthalene-1,5-disulfonate |
|---|---|
| Formula | C22 H26 N4 Ni O8 S2 |
| Calculated formula | C22 H26 N4 Ni O8 S2 |
| Title of publication | Synthesis, crystal structure and Hirshfeld surface analysis of di-aqua-bis-(<i>o</i>-phenyl-enedi-amine-κ<sup>2</sup><i>N</i>,<i>N</i>')nickel(II) naphthalene-1,5-di-sulfonate. |
| Authors of publication | Suyunov, Jabbor R.; Turaev, Khayit Kh; Alimnazarov, Bekmurod Kh; Nazarov, Yusuf E.; Mengnorov, Islombek J.; Ibragimov, Bakhtiyar T.; Ashurov, Jamshid M. |
| Journal of publication | Acta crystallographica. Section E, Crystallographic communications |
| Year of publication | 2023 |
| Journal volume | 79 |
| Journal issue | Pt 11 |
| Pages of publication | 1083 - 1087 |
| a | 12.7613 ± 0.0003 Å |
| b | 7.7054 ± 0.0001 Å |
| c | 13.4641 ± 0.0003 Å |
| α | 90° |
| β | 111.554 ± 0.002° |
| γ | 90° |
| Cell volume | 1231.36 ± 0.05 Å3 |
| Cell temperature | 563.15 K |
| Ambient diffraction temperature | 563.15 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0391 |
| Residual factor for significantly intense reflections | 0.036 |
| Weighted residual factors for significantly intense reflections | 0.0948 |
| Weighted residual factors for all reflections included in the refinement | 0.0971 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.044 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 288137 (current) | 2023-12-07 | cif/ Updating files of 2022926 Original log message: Adding full bibliography for 2022926.cif. |
2022926.cif 2022926.hkl |
| 287136 | 2023-10-27 | cif/ hkl/ Adding structures of 2022926 via cif-deposit CGI script. |
2022926.cif 2022926.hkl |
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