Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 2232469
Preview
| Coordinates | 2232469.cif |
|---|---|
| Structure factors | 2232469.hkl |
| Original IUCr paper | HTML |
| Chemical name | <i>catena</i>-Poly[[lead(II)-μ-(2-oxidobenzaldehyde isonicotinoylhydrazonato)] methanol monosolvate] |
|---|---|
| Formula | C14 H13 N3 O3 Pb |
| Calculated formula | C14 H13 N3 O3 Pb |
| SMILES | [Pb]12(Oc3ccccc3C=[N]2N=C(O1)c1ccncc1)[n]1ccc(C2O[Pb]3Oc4ccccc4C=[N]3N=2)cc1.OC.OC |
| Title of publication | <i>catena</i>-Poly[[lead(II)-μ-(2-oxidobenzaldehyde isonicotinoylhydrazonato)] methanol monosolvate] |
| Authors of publication | Shahverdizadeh, Gholam Hossein; Ng, Seik Weng; Tiekink, Edward R. T.; Mirtamizdoust, Babak |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2011 |
| Journal volume | 67 |
| Journal issue | 11 |
| Pages of publication | m1583 |
| a | 28.6702 ± 0.0005 Å |
| b | 28.6702 ± 0.0005 Å |
| c | 9.0146 ± 0.0002 Å |
| α | 90° |
| β | 90° |
| γ | 120° |
| Cell volume | 6417.1 ± 0.2 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 148 |
| Hermann-Mauguin space group symbol | R -3 :H |
| Hall space group symbol | -R 3 |
| Residual factor for all reflections | 0.0161 |
| Residual factor for significantly intense reflections | 0.0146 |
| Weighted residual factors for significantly intense reflections | 0.0318 |
| Weighted residual factors for all reflections included in the refinement | 0.0322 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.108 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 181246 (current) | 2016-04-03 | hkl/2/23/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/23/24. |
2232469.cif 2232469.hkl |
| 176798 | 2016-02-21 | cif/2/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/23. |
2232469.cif 2232469.hkl |
| 120072 | 2014-07-11 | Adding DOIs to range 2 structures. | 2232469.cif 2232469.hkl |
| 88064 | 2013-08-29 | Adding _cod_database_fobs_code data item to all COD CIFs that have Fobs deposited and did not have this data item yet. | 2232469.cif 2232469.hkl |
| 31968 | 2012-01-03 | hkl/ Adding automatically assigned IUCr Fobs data for the rest of the year 2001 structures. |
2232469.cif 2232469.hkl |
| 31131 | 2011-12-12 | ../uploads/cif-deposit/cod/cif Adding structures of 2232469 via cif-deposit CGI script. |
2232469.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.