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Information card for entry 2232706
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| Coordinates | 2232706.cif |
|---|---|
| Structure factors | 2232706.hkl |
| Original IUCr paper | HTML |
| Chemical name | Bis{1,2-bis[bis(3-methoxypropyl)phosphanyl]ethane-\ κ^2^<i>P</i>,<i>P</i>'}dichloridoosmium(II) |
|---|---|
| Formula | C36 H80 Cl2 O8 Os P4 |
| Calculated formula | C36 H80 Cl2 O8 Os P4 |
| Title of publication | Bis{1,2-bis[bis(3-methoxypropyl)phosphanyl]ethane-κ^2^<i>P</i>,<i>P</i>'}dichloridoosmium(II) |
| Authors of publication | Szymczak, Nathaniel K.; Zakharov, Lev N.; Tyler, David R. |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2011 |
| Journal volume | 67 |
| Journal issue | 12 |
| Pages of publication | m1808 |
| a | 12.667 ± 0.003 Å |
| b | 10.321 ± 0.002 Å |
| c | 18.754 ± 0.004 Å |
| α | 90° |
| β | 107.779 ± 0.003° |
| γ | 90° |
| Cell volume | 2334.7 ± 0.9 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0339 |
| Residual factor for significantly intense reflections | 0.0244 |
| Weighted residual factors for significantly intense reflections | 0.0531 |
| Weighted residual factors for all reflections included in the refinement | 0.0579 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.043 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 181249 (current) | 2016-04-03 | hkl/2/23/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/23/27. |
2232706.cif 2232706.hkl |
| 176798 | 2016-02-21 | cif/2/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/23. |
2232706.cif 2232706.hkl |
| 120072 | 2014-07-11 | Adding DOIs to range 2 structures. | 2232706.cif 2232706.hkl |
| 88064 | 2013-08-29 | Adding _cod_database_fobs_code data item to all COD CIFs that have Fobs deposited and did not have this data item yet. | 2232706.cif 2232706.hkl |
| 31968 | 2012-01-03 | hkl/ Adding automatically assigned IUCr Fobs data for the rest of the year 2001 structures. |
2232706.cif 2232706.hkl |
| 31584 | 2012-01-02 | ../uploads/cif-deposit/cod/cif Adding structures of 2232706 via cif-deposit CGI script. |
2232706.cif |
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Users of the data should acknowledge the original authors of the
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