Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 2234744
Preview
| Coordinates | 2234744.cif |
|---|---|
| Structure factors | 2234744.hkl |
| Original IUCr paper | HTML |
| Chemical name | Poly[[tris(μ-4,4'-bipyridine-κ^2^<i>N</i>:<i>N</i>')bis(μ-<i>L</i>- lysinato-κ^3^<i>N</i>^1^,<i>O</i>^1^:<i>O</i>^1'^)dizinc(II)] tetranitrate 0.6-hydrate dimethylformamide disolvate] |
|---|---|
| Formula | C48 H67.2 N16 O18.6 Zn2 |
| Calculated formula | C48 H67.2 N16 O18.6 Zn2 |
| Title of publication | Poly[[tris(μ-4,4'-bipyridine-κ^2^<i>N</i>:<i>N</i>')bis(μ-<small>L</small>-lysinato-κ^3^<i>N</i>^1^,<i>O</i>^1^:<i>O</i>^1'^)dizinc(II)] tetranitrate 0.6-hydrate dimethylformamide disolvate] |
| Authors of publication | Li, Shu-Qiang; Hu, Ning-Hai |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2012 |
| Journal volume | 68 |
| Journal issue | 5 |
| Pages of publication | m633 - m634 |
| a | 10.3039 ± 0.0004 Å |
| b | 24.9425 ± 0.001 Å |
| c | 11.574 ± 0.0004 Å |
| α | 90° |
| β | 93.197 ± 0.001° |
| γ | 90° |
| Cell volume | 2969.95 ± 0.19 Å3 |
| Cell temperature | 187 ± 2 K |
| Ambient diffraction temperature | 187 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for all reflections | 0.0464 |
| Residual factor for significantly intense reflections | 0.0414 |
| Weighted residual factors for significantly intense reflections | 0.1032 |
| Weighted residual factors for all reflections included in the refinement | 0.1067 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.003 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 181269 (current) | 2016-04-03 | hkl/2/23/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/23/47. |
2234744.cif 2234744.hkl |
| 176435 | 2016-02-14 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries from ranges 1, 2. |
2234744.cif 2234744.hkl |
| 120072 | 2014-07-11 | Adding DOIs to range 2 structures. | 2234744.cif 2234744.hkl |
| 88064 | 2013-08-29 | Adding _cod_database_fobs_code data item to all COD CIFs that have Fobs deposited and did not have this data item yet. | 2234744.cif 2234744.hkl |
| 66590 | 2012-09-11 | hkl/ Adding assigned .htl files for the most recent IUCr data depositions. |
2234744.cif 2234744.hkl |
| 60243 | 2012-06-14 | cif/ Adding structures of 2234744 via cif-deposit CGI script. |
2234744.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.