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Information card for entry 2237540
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| Coordinates | 2237540.cif |
|---|---|
| Structure factors | 2237540.hkl |
| Original IUCr paper | HTML |
| Chemical name | Chlorido[2,3,5,6-tetrakis(<i>tert</i>-butylsulfanylmethyl)phenyl-κ^3^<i>S</i>^2^,<i>C</i>^1^,<i>S</i>^6^]palladium(II) dichloromethane monosolvate |
|---|---|
| Formula | C27 H47 Cl3 Pd S4 |
| Calculated formula | C27 H47 Cl3 Pd S4 |
| Title of publication | Chlorido[2,3,5,6-tetrakis(<i>tert</i>-butylsulfanylmethyl)phenyl-κ^3^<i>S</i>^2^,<i>C</i>^1^,<i>S</i>^6^]palladium(II) dichloromethane monosolvate |
| Authors of publication | Paz-Morales, Evelyn; Hernández-Ortega, Simón; Morales-Morales, David |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2013 |
| Journal volume | 69 |
| Journal issue | 3 |
| Pages of publication | m139 - m140 |
| a | 15.917 ± 0.015 Å |
| b | 13.768 ± 0.013 Å |
| c | 17.808 ± 0.016 Å |
| α | 90° |
| β | 105.216 ± 0.015° |
| γ | 90° |
| Cell volume | 3766 ± 6 Å3 |
| Cell temperature | 298 ± 2 K |
| Ambient diffraction temperature | 298 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0676 |
| Residual factor for significantly intense reflections | 0.0476 |
| Weighted residual factors for significantly intense reflections | 0.1026 |
| Weighted residual factors for all reflections included in the refinement | 0.1098 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.026 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 181297 (current) | 2016-04-03 | hkl/2/23/ (antanas@echidna) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/23/75. |
2237540.cif 2237540.hkl |
| 176798 | 2016-02-21 | cif/2/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 2/23. |
2237540.cif 2237540.hkl |
| 88055 | 2013-08-28 | cod/cif/ (saulius@koala.ibt.lt) Adding the _cod_database_fobs_code links for those COD CIFs that have their Fobs deposited recently. |
2237540.cif 2237540.hkl |
| 88054 | 2013-08-28 | cod/hkl/ (saulius@koala.ibt.lt) Adding Fobs files for the recently deposited IUCr coordinate data. |
2237540.cif 2237540.hkl |
| 78834 | 2013-04-02 | cif/ Adding structures of 2237540 via cif-deposit CGI script. |
2237540.cif |
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Users of the data should acknowledge the original authors of the
structural data.