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Information card for entry 2243146
Preview
| Coordinates | 2243146.cif |
|---|---|
| Structure factors | 2243146.hkl |
| Original IUCr paper | HTML |
| Chemical name | <i>catena</i>-Poly[[[(1,3-dibenzyl-4,5-diphenyl-2-selenoimidazole-κ<i>Se</i>)copper(I)]-μ-cyanido-κ^2^<i>C</i>:<i>N</i>] acetonitrile monosolvate] |
|---|---|
| Formula | C32 H27 Cu N4 Se |
| Calculated formula | C32 H27 Cu N4 Se |
| Title of publication | Unexpected reactions of NHC*—Cu^I^ and —Ag^I^ bromides with potassium thio- or selenocyanate |
| Authors of publication | Tacke, Matthias; Marhöfer, Daniel; Althani, Hessah; Müller-Bunz, Helge |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2019 |
| Journal volume | 75 |
| Journal issue | 11 |
| Pages of publication | 1657 - 1663 |
| a | 13.7704 ± 0.0003 Å |
| b | 14.3398 ± 0.0003 Å |
| c | 28.4102 ± 0.0007 Å |
| α | 90° |
| β | 93.024 ± 0.002° |
| γ | 90° |
| Cell volume | 5602.2 ± 0.2 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0546 |
| Residual factor for significantly intense reflections | 0.048 |
| Weighted residual factors for significantly intense reflections | 0.1156 |
| Weighted residual factors for all reflections included in the refinement | 0.1193 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.062 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 219488 (current) | 2019-10-24 | cif/ hkl/ Adding structures of 2243144, 2243145, 2243146 via cif-deposit CGI script. |
2243146.cif 2243146.hkl |
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Users of the data should acknowledge the original authors of the
structural data.