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Information card for entry 2243517
Preview
| Coordinates | 2243517.cif |
|---|---|
| Structure factors | 2243517.hkl |
| Original IUCr paper | HTML |
| Chemical name | Poly[[μ~3~-acetato-hexakis(μ-<i>N</i>,<i>N</i>-dimethylformamide)bis(<i>N</i>,<i>N</i>-dimethylformamide)bis[salicylhydroximato(2-)]heptakis[salicylhydroximato(3-)]hexaaluminium(III)dysprosium(III)pentasodium(I)] <i>N</i>,<i>N</i>-dimethylformamide tetrasolvate monohydrate] |
|---|---|
| Formula | C101 H127 Al6 Dy N21 Na5 O42 |
| Calculated formula | C101 H127 Al6 Dy N21 Na5 O42 |
| Title of publication | Crystal structures of two dysprosium‒aluminium‒sodium [3.3.1] metallacryptates that form two-dimensional sheets |
| Authors of publication | Travis, Jordan R.; Van Trieste III, Gerard P.; Zeller, Matthias; Zaleski, Curtis M. |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2020 |
| Journal volume | 76 |
| Journal issue | 8 |
| Pages of publication | 1378 - 1390 |
| a | 22.6809 ± 0.0013 Å |
| b | 20.5788 ± 0.0011 Å |
| c | 27.6206 ± 0.0016 Å |
| α | 90° |
| β | 101.59 ± 0.002° |
| γ | 90° |
| Cell volume | 12628.9 ± 1.2 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 9 |
| Hermann-Mauguin space group symbol | C 1 c 1 |
| Hall space group symbol | C -2yc |
| Residual factor for all reflections | 0.0718 |
| Residual factor for significantly intense reflections | 0.0561 |
| Weighted residual factors for significantly intense reflections | 0.1463 |
| Weighted residual factors for all reflections included in the refinement | 0.1588 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.05 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 254730 (current) | 2020-08-01 | cif/ hkl/ Adding structures of 2243517, 2243518 via cif-deposit CGI script. |
2243517.cif 2243517.hkl |
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Users of the data should acknowledge the original authors of the
structural data.