Crystallography Open Database

Information card for entry 2243518

Preview

Coordinates	2243518.cif
Structure factors	2243518.hkl
Original paper (by DOI)	HTML

Structure parameters

Chemical name	Poly[[di-μ~4~-acetato-nonakis(μ-<i>N</i>,<i>N</i>-dimethylformamide)octakis(<i>N</i>,<i>N</i>-dimethylformamide)tetrakis[salicylhydroximato(2-)]tetradecakis[salicylhydroximato(3-)]dodecaaluminium(III)didysprosium(III)decasodium(I)] <i>N</i>,<i>N</i>-dimethylformamide 6.335-solvate]
Formula	C200.01 H245.35 Al12 Dy2 N41.34 Na10 O81.34
Calculated formula	C200.005 H245.345 Al12 Dy2 N41.335 Na10 O81.335
Title of publication	Crystal structures of two dysprosium‒aluminium‒sodium [3.3.1] metallacryptates that form two-dimensional sheets
Authors of publication	Travis, Jordan R.; Van Trieste III, Gerard P.; Zeller, Matthias; Zaleski, Curtis M.
Journal of publication	Acta Crystallographica Section E
Year of publication	2020
Journal volume	76
Journal issue	8
Pages of publication	1378 - 1390
a	28.1847 ± 0.0014 Å
b	15.3683 ± 0.0008 Å
c	30.7354 ± 0.0016 Å
α	90°
β	106.461 ± 0.002°
γ	90°
Cell volume	12767.4 ± 1.1 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	7
Hermann-Mauguin space group symbol	P 1 c 1
Hall space group symbol	P -2yc
Residual factor for all reflections	0.0557
Residual factor for significantly intense reflections	0.0527
Weighted residual factors for significantly intense reflections	0.1351
Weighted residual factors for all reflections included in the refinement	0.1374
Goodness-of-fit parameter for all reflections included in the refinement	1.02
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	Yes

Version history

Revision	Date	Message	Files
254730 (current)	2020-08-01	cif/ hkl/ Adding structures of 2243517, 2243518 via cif-deposit CGI script.	2243518.cif 2243518.hkl