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Information card for entry 4066933
Preview
| Coordinates | 4066933.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C21 H46 O3 Si5 |
|---|---|
| Calculated formula | C21 H46 O3 Si5 |
| SMILES | C[Si](C)(C)[Si](C[Si](C)(C)c1c(cc(cc1OC)OC)OC)([Si](C)(C)C)[Si](C)(C)C |
| Title of publication | Synthesis and Characterization of {[Tris(trimethylsilyl)silyl]methyl}silanes of the Formula Type Me4−nSi[CH2Si(SiMe3)3]n(n= 1−3) and Derivatives |
| Authors of publication | Berkefeld, André; Troegel, Dennis; Burschka, Christian; Tacke, Reinhold |
| Journal of publication | Organometallics |
| Year of publication | 2010 |
| Journal volume | 29 |
| Journal issue | 20 |
| Pages of publication | 4548 |
| a | 9.8311 ± 0.0013 Å |
| b | 11.0157 ± 0.0013 Å |
| c | 15.9346 ± 0.0019 Å |
| α | 79.739 ± 0.014° |
| β | 84.82 ± 0.015° |
| γ | 63.886 ± 0.013° |
| Cell volume | 1524.6 ± 0.4 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0539 |
| Residual factor for significantly intense reflections | 0.0387 |
| Weighted residual factors for significantly intense reflections | 0.104 |
| Weighted residual factors for all reflections included in the refinement | 0.1161 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.069 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178561 (current) | 2016-03-21 | cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/69. |
4066933.cif |
| 91935 | 2013-12-29 | cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs. |
4066933.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4066933.cif |
| 34027 | 2012-02-13 | ../uploads/cif-deposit/cod/cif Adding structures of 4066931, 4066932, 4066933, 4066934, 4066935 via cif-deposit CGI script. |
4066933.cif |
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Users of the data should acknowledge the original authors of the
structural data.