Crystallography Open Database

Information card for entry 4066934

Preview

Coordinates	4066934.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H72 O3 Si9
Calculated formula	C30 H72 O3 Si9
Title of publication	Synthesis and Characterization of {[Tris(trimethylsilyl)silyl]methyl}silanes of the Formula Type Me4−nSi[CH2Si(SiMe3)3]n(n= 1−3) and Derivatives
Authors of publication	Berkefeld, André; Troegel, Dennis; Burschka, Christian; Tacke, Reinhold
Journal of publication	Organometallics
Year of publication	2010
Journal volume	29
Journal issue	20
Pages of publication	4548
a	10.017 ± 0.002 Å
b	26.789 ± 0.004 Å
c	10.0531 ± 0.0017 Å
α	90°
β	118.64 ± 0.02°
γ	90°
Cell volume	2367.6 ± 0.8 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	4
Space group number	6
Hermann-Mauguin space group symbol	P 1 m 1
Hall space group symbol	P -2y
Residual factor for all reflections	0.0509
Residual factor for significantly intense reflections	0.0464
Weighted residual factors for significantly intense reflections	0.1285
Weighted residual factors for all reflections included in the refinement	0.1314
Goodness-of-fit parameter for all reflections included in the refinement	1.06
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178561 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/69.	4066934.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4066934.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4066934.cif
34027	2012-02-13	../uploads/cif-deposit/cod/cif Adding structures of 4066931, 4066932, 4066933, 4066934, 4066935 via cif-deposit CGI script.	4066934.cif