Crystallography Open Database

Information card for entry 4069922

Preview

Coordinates	4069922.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H43 Ge2 P2 Pt
Calculated formula	C33.5 H41.5 Ge2 P2 Pt
Title of publication	Formation and Ring Expansion of Germaplatinacycles via Dehydrogenative Ge−Ge and Ge−Pt Bond-Forming Reactions
Authors of publication	Tanabe, Makoto; Hanzawa, Masaya; Ishikawa, Naoko; Osakada, Kohtaro
Journal of publication	Organometallics
Year of publication	2009
Journal volume	28
Journal issue	20
Pages of publication	6014
a	17.672 ± 0.004 Å
b	11.87 ± 0.002 Å
c	17.501 ± 0.003 Å
α	90°
β	118.373 ± 0.003°
γ	90°
Cell volume	3230.1 ± 1.1 Å³
Cell temperature	113.1 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0386
Residual factor for significantly intense reflections	0.0351
Weighted residual factors for significantly intense reflections	0.0938
Weighted residual factors for all reflections included in the refinement	0.0963
Goodness-of-fit parameter for all reflections included in the refinement	1.044
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4069922.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4069922.cif
40512	2012-03-07	../uploads/cif-deposit/cod/cif Adding structures of 4069922, 4069923, 4069924 via cif-deposit CGI script.	4069922.cif