Crystallography Open Database

Information card for entry 4070714

Preview

Coordinates	4070714.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C55 H66 N3 P Rh Si4 Sn
Calculated formula	C55 H66 N3 P Rh Si4 Sn
Title of publication	Triamidostannates(II) as Sterically Demanding Ligands for Rhodium and Iridium
Authors of publication	Kilian, Michaela; Wadepohl, Hubert; Gade, Lutz H.
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	4
Pages of publication	524
a	11.87 ± 0.003 Å
b	11.947 ± 0.002 Å
c	19.451 ± 0.005 Å
α	85.419 ± 0.005°
β	81.054 ± 0.004°
γ	81.686 ± 0.004°
Cell volume	2691.5 ± 1.1 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.058
Residual factor for significantly intense reflections	0.0376
Weighted residual factors for significantly intense reflections	0.0692
Weighted residual factors for all reflections included in the refinement	0.0744
Goodness-of-fit parameter for all reflections included in the refinement	1.048
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178596 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/07.	4070714.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4070714.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4070714.cif
42655	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 4070709, 4070710, 4070711, 4070712, 4070713, 4070714, 4070715 via cif-deposit CGI script.	4070714.cif