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Information card for entry 4070715
Preview
| Coordinates | 4070715.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C54 H69 Ir N3 P Si4 Sn |
|---|---|
| Calculated formula | C54 H69 Ir N3 P Si4 Sn |
| SMILES | [CH]12=[CH]3CC[CH]4=[CH](CC1)[IrH]1234(c2c(ccc(c2)C)N2[Si](C)(C)[Si]3(C)[Si](C)(C)N(c4ccc(cc4)C)[Sn]12N(c1ccc(cc1)C)[Si]3(C)C)[P](c1ccccc1)(c1ccccc1)c1ccccc1 |
| Title of publication | Triamidostannates(II) as Sterically Demanding Ligands for Rhodium and Iridium |
| Authors of publication | Kilian, Michaela; Wadepohl, Hubert; Gade, Lutz H. |
| Journal of publication | Organometallics |
| Year of publication | 2008 |
| Journal volume | 27 |
| Journal issue | 4 |
| Pages of publication | 524 |
| a | 12.91 ± 0.005 Å |
| b | 16.198 ± 0.008 Å |
| c | 28.002 ± 0.009 Å |
| α | 90° |
| β | 115.862 ± 0.019° |
| γ | 90° |
| Cell volume | 5269 ± 4 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0486 |
| Residual factor for significantly intense reflections | 0.0348 |
| Weighted residual factors for significantly intense reflections | 0.0795 |
| Weighted residual factors for all reflections included in the refinement | 0.0853 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.087 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178596 (current) | 2016-03-21 | cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/07. |
4070715.cif |
| 120075 | 2014-07-11 | Adding DOIs to range 4/07 structures. | 4070715.cif |
| 47256 | 2012-03-23 | cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories. |
4070715.cif |
| 42655 | 2012-03-13 | ../uploads/cif-deposit/cod/cif Adding structures of 4070709, 4070710, 4070711, 4070712, 4070713, 4070714, 4070715 via cif-deposit CGI script. |
4070715.cif |
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Users of the data should acknowledge the original authors of the
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