Crystallography Open Database

Information card for entry 4070716

Preview

Coordinates	4070716.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	octakis(3-chloropropanyl-sesquisiloxane)
Formula	C24 H48 Cl8 O12 Si8
Calculated formula	C24 H48 Cl8 O12 Si8
Title of publication	New, Effective Method of Synthesis and Structural Characterization of Octakis(3-chloropropyl)octasilsesquioxane
Authors of publication	Marciniec, Bogdan; Dutkiewicz, Michal; Maciejewski, Hieronim; Kubicki, Maciej
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	4
Pages of publication	793
a	10.02 ± 0.003 Å
b	10.133 ± 0.003 Å
c	12.855 ± 0.005 Å
α	79.93 ± 0.03°
β	73.96 ± 0.03°
γ	78.09 ± 0.03°
Cell volume	1217.7 ± 0.7 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1604
Residual factor for significantly intense reflections	0.0859
Weighted residual factors for significantly intense reflections	0.1976
Weighted residual factors for all reflections included in the refinement	0.2105
Goodness-of-fit parameter for all reflections included in the refinement	1.768
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178596 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/07.	4070716.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4070716.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4070716.cif
42656	2012-03-13	../uploads/cif-deposit/cod/cif Adding structures of 4070716 via cif-deposit CGI script.	4070716.cif