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Information card for entry 4071066
Preview
| Coordinates | 4071066.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | MeSi(phac-Rh(COD))3 |
|---|---|
| Chemical name | tris(1,5-cyclooctadiene)[mu-[3,3',3"-[methylsilylidynetris(1,4- phenylene)]tris(2,4-pentanedionato)]trirhodium toluene solvate |
| Formula | C65 H77 O6 Rh3 Si |
| Calculated formula | C65 H74 O6 Rh3 Si |
| Title of publication | Organosilicon-Based Multifunctional β-Diketones and their Rhodium and Iridium Complexes |
| Authors of publication | Pariya, Chandi; Marcos, Yoseph S.; Zhang, Yixun; Fronczek, Frank R.; Maverick, Andrew W. |
| Journal of publication | Organometallics |
| Year of publication | 2008 |
| Journal volume | 27 |
| Journal issue | 17 |
| Pages of publication | 4318 |
| a | 6.8596 ± 0.001 Å |
| b | 16.044 ± 0.003 Å |
| c | 27.2 ± 0.005 Å |
| α | 98.156 ± 0.007° |
| β | 96.646 ± 0.009° |
| γ | 97.498 ± 0.009° |
| Cell volume | 2910.3 ± 0.9 Å3 |
| Cell temperature | 90 K |
| Ambient diffraction temperature | 90 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.119 |
| Residual factor for significantly intense reflections | 0.06 |
| Weighted residual factors for significantly intense reflections | 0.118 |
| Weighted residual factors for all reflections included in the refinement | 0.138 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.022 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178599 (current) | 2016-03-21 | cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/10. |
4071066.cif |
| 91935 | 2013-12-29 | cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs. |
4071066.cif |
| 47256 | 2012-03-23 | cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories. |
4071066.cif |
| 43021 | 2012-03-13 | ../uploads/cif-deposit/cod/cif Adding structures of 4071061, 4071062, 4071063, 4071064, 4071065, 4071066, 4071067 via cif-deposit CGI script. |
4071066.cif |
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Users of the data should acknowledge the original authors of the
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