Crystallography Open Database

Information card for entry 4072154

Preview

Coordinates	4072154.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H48 N Si2 U
Calculated formula	C26 H47 N Si2 U
Title of publication	A Mild Protocol To Generate Uranium(IV) Mixed-Ligand Metallocene Complexes using Copper(I) Iodide
Authors of publication	Graves, Christopher R.; Schelter, Eric J.; Cantat, Thibault; Scott, Brian L.; Kiplinger, Jaqueline L.
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	20
Pages of publication	5371
a	8.753 ± 0.003 Å
b	15.573 ± 0.005 Å
c	11.017 ± 0.003 Å
α	90°
β	110.86°
γ	90°
Cell volume	1403.3 ± 0.8 Å³
Cell temperature	120 ± 1 K
Ambient diffraction temperature	120 ± 1 K
Number of distinct elements	5
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.1049
Residual factor for significantly intense reflections	0.0787
Weighted residual factors for significantly intense reflections	0.2064
Weighted residual factors for all reflections included in the refinement	0.2123
Goodness-of-fit parameter for all reflections included in the refinement	1.539
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178610 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/21.	4072154.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4072154.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4072154.cif
44265	2012-03-15	../uploads/cif-deposit/cod/cif Adding structures of 4072151, 4072152, 4072153, 4072154, 4072155 via cif-deposit CGI script.	4072154.cif