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Information card for entry 4072155
Preview
Coordinates | 4072155.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C32 H44 N U |
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Calculated formula | C32 H39 N U |
SMILES | [U]123456789(N(c%10c9cccc%10)c9ccccc9)([c]9([c]1([c]8([c]2([c]39C)C)C)C)C)[c]1([c]4([c]5([c]6([c]71C)C)C)C)C |
Title of publication | A Mild Protocol To Generate Uranium(IV) Mixed-Ligand Metallocene Complexes using Copper(I) Iodide |
Authors of publication | Graves, Christopher R.; Schelter, Eric J.; Cantat, Thibault; Scott, Brian L.; Kiplinger, Jaqueline L. |
Journal of publication | Organometallics |
Year of publication | 2008 |
Journal volume | 27 |
Journal issue | 20 |
Pages of publication | 5371 |
a | 9.2465 ± 0.0009 Å |
b | 10.885 ± 0.0011 Å |
c | 13.7791 ± 0.0014 Å |
α | 86.5926 ± 0.0014° |
β | 80.0815 ± 0.0014° |
γ | 80.0828 ± 0.0015° |
Cell volume | 1345.1 ± 0.2 Å3 |
Cell temperature | 120 ± 1 K |
Ambient diffraction temperature | 120 ± 1 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0441 |
Residual factor for significantly intense reflections | 0.0374 |
Weighted residual factors for significantly intense reflections | 0.0842 |
Weighted residual factors for all reflections included in the refinement | 0.0875 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.826 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
178610 (current) | 2016-03-21 | cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/21. |
4072155.cif |
91935 | 2013-12-29 | cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs. |
4072155.cif |
47256 | 2012-03-23 | cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories. |
4072155.cif |
44265 | 2012-03-15 | ../uploads/cif-deposit/cod/cif Adding structures of 4072151, 4072152, 4072153, 4072154, 4072155 via cif-deposit CGI script. |
4072155.cif |
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Users of the data should acknowledge the original authors of the
structural data.