Crystallography Open Database

Information card for entry 4072661

Preview

Coordinates	4072661.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H60 N4 O3 Os2 Pd Si4
Calculated formula	C30 H60 N4 O3 Os2 Pd Si4
Title of publication	Synthesis, Structure, and Reactivity of Organometallic Osmium(VI) Hydroxo Compounds
Authors of publication	Kiefer, Adam M.; Giles, John A.; Shapley, Patricia A.
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	8
Pages of publication	1881
a	12.35 ± 0.0009 Å
b	18.3598 ± 0.0013 Å
c	19.9189 ± 0.0013 Å
α	90°
β	101.883 ± 0.003°
γ	90°
Cell volume	4419.7 ± 0.5 Å³
Cell temperature	297 ± 2 K
Ambient diffraction temperature	297 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0624
Residual factor for significantly intense reflections	0.0327
Weighted residual factors for significantly intense reflections	0.0641
Weighted residual factors for all reflections included in the refinement	0.0769
Goodness-of-fit parameter for all reflections included in the refinement	1.02
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176432 (current)	2016-02-14	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries.	4072661.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4072661.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4072661.cif
45939	2012-03-21	../uploads/cif-deposit/cod/cif Adding structures of 4072661 via cif-deposit CGI script.	4072661.cif