Crystallography Open Database

Information card for entry 4072662

Preview

Coordinates	4072662.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H60 N2 O2 Os Si2
Calculated formula	C24 H60 N2 O2 Os Si2
SMILES	[Os](O)(O)(#N)(C[Si](C)(C)C)C[Si](C)(C)C.[N+](CCCC)(CCCC)(CCCC)CCCC
Title of publication	Synthesis, Structure, and Reactivity of Organometallic Osmium(VI) Hydroxo Compounds
Authors of publication	Kiefer, Adam M.; Giles, John A.; Shapley, Patricia A.
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	8
Pages of publication	1881
a	15.045 ± 0.006 Å
b	19.289 ± 0.008 Å
c	22.687 ± 0.009 Å
α	90°
β	90°
γ	90°
Cell volume	6584 ± 5 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	6
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.1715
Residual factor for significantly intense reflections	0.0697
Weighted residual factors for significantly intense reflections	0.0983
Weighted residual factors for all reflections included in the refinement	0.1191
Goodness-of-fit parameter for all reflections included in the refinement	0.993
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176432 (current)	2016-02-14	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries.	4072662.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4072662.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4072662.cif
45940	2012-03-21	../uploads/cif-deposit/cod/cif Adding structures of 4072662 via cif-deposit CGI script.	4072662.cif