Crystallography Open Database

Information card for entry 4072716

Preview

Coordinates	4072716.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	Bis[μ~3~-1,1,2,2-tetrakis(trimethylsilyl)disilane-1,2-diolato- 1:2K^2^O;2:3K^2^O']-pentamethyltrialuminium
Formula	C29 H87 Al3 O4 Si12
Calculated formula	C29 H87 Al3 O4 Si12
Title of publication	Synthesis and Structure of Cyclic Aluminum Disiloxides
Authors of publication	Krempner, C.; Reinke, H.; Weichert, K.
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	6
Pages of publication	1386
a	13.4937 ± 0.0003 Å
b	13.4937 ± 0.0003 Å
c	35.3988 ± 0.0009 Å
α	90°
β	90°
γ	90°
Cell volume	6445.4 ± 0.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	96
Hermann-Mauguin space group symbol	P 43 21 2
Hall space group symbol	P 4nw 2abw
Residual factor for all reflections	0.0709
Residual factor for significantly intense reflections	0.0563
Weighted residual factors for significantly intense reflections	0.1535
Weighted residual factors for all reflections included in the refinement	0.1651
Goodness-of-fit parameter for all reflections included in the refinement	1.045
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176432 (current)	2016-02-14	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries.	4072716.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4072716.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4072716.cif
45966	2012-03-21	../uploads/cif-deposit/cod/cif Adding structures of 4072714, 4072715, 4072716, 4072717, 4072718 via cif-deposit CGI script.	4072716.cif