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Information card for entry 4072717
Preview
| Coordinates | 4072717.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Chemical name | (4R*,5R*)-2,4,5-Trimethyl-4,5-bis[tris(trimethylsilyl)silyl]- 2-alumina-1,3-dioxa-4,5-disilacylopentane-tetrahydrofuranate |
|---|---|
| Formula | C25 H71 Al O3 Si10 |
| Calculated formula | C25 H71 Al O3 Si10 |
| SMILES | [Al]1(O[Si]([Si]([Si]([Si](C)(C)C)([Si](C)(C)C)[Si](C)(C)C)(O1)C)([Si]([Si](C)(C)C)([Si](C)(C)C)[Si](C)(C)C)C)([O]1CCCC1)C |
| Title of publication | Synthesis and Structure of Cyclic Aluminum Disiloxides |
| Authors of publication | Krempner, C.; Reinke, H.; Weichert, K. |
| Journal of publication | Organometallics |
| Year of publication | 2007 |
| Journal volume | 26 |
| Journal issue | 6 |
| Pages of publication | 1386 |
| a | 9.5867 ± 0.0003 Å |
| b | 13.3815 ± 0.0004 Å |
| c | 18.9958 ± 0.0005 Å |
| α | 106.757 ± 0.001° |
| β | 98.152 ± 0.001° |
| γ | 94.488 ± 0.001° |
| Cell volume | 2291.49 ± 0.12 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.046 |
| Residual factor for significantly intense reflections | 0.0356 |
| Weighted residual factors for significantly intense reflections | 0.0927 |
| Weighted residual factors for all reflections included in the refinement | 0.1008 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.012 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178616 (current) | 2016-03-21 | cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/27. |
4072717.cif |
| 120075 | 2014-07-11 | Adding DOIs to range 4/07 structures. | 4072717.cif |
| 47256 | 2012-03-23 | cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories. |
4072717.cif |
| 45966 | 2012-03-21 | ../uploads/cif-deposit/cod/cif Adding structures of 4072714, 4072715, 4072716, 4072717, 4072718 via cif-deposit CGI script. |
4072717.cif |
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Users of the data should acknowledge the original authors of the
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