Crystallography Open Database

Information card for entry 4074070

Preview

Coordinates	4074070.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C19 H29 Co Si
Calculated formula	C19 H29 Co Si
SMILES	[Co]12345678[cH]9[cH]7[cH]8[cH]5[c]19[Si](C[C]14=[C]2([C]6(=[C]31C)C)C)(C(C)C)C(C)C
Title of publication	Synthesis of Neutral Mixed Sandwich CH2-SiR2Bridged [2]Cobaltoarenophanes from the Dilithiation of Cb*CoCp [Co(η4-C4Me4)(η5-C5H5)]
Authors of publication	Chadha, Preeti; Dutton, Jason L.; Sgro, Michael J.; Ragogna, Paul J.
Journal of publication	Organometallics
Year of publication	2007
Journal volume	26
Journal issue	25
Pages of publication	6063
a	12.898 ± 0.003 Å
b	17.481 ± 0.004 Å
c	8.2913 ± 0.0017 Å
α	90°
β	103.99 ± 0.03°
γ	90°
Cell volume	1814 ± 0.7 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0403
Residual factor for significantly intense reflections	0.035
Weighted residual factors for significantly intense reflections	0.0955
Weighted residual factors for all reflections included in the refinement	0.0986
Goodness-of-fit parameter for all reflections included in the refinement	1.064
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178629 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/40.	4074070.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4074070.cif
47256	2012-03-23	cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories.	4074070.cif
46717	2012-03-21	../uploads/cif-deposit/cod/cif Adding structures of 4074070, 4074071 via cif-deposit CGI script.	4074070.cif