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Information card for entry 4074071
Preview
| Coordinates | 4074071.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C15 H21 Co Si |
|---|---|
| Calculated formula | C15 H21 Co Si |
| SMILES | [Co]12345678[C]9(=[C]1([C]2(=[C]39C)C)C)C[Si](C)(C)[c]14[cH]5[cH]6[cH]7[cH]81 |
| Title of publication | Synthesis of Neutral Mixed Sandwich CH2-SiR2Bridged [2]Cobaltoarenophanes from the Dilithiation of Cb*CoCp [Co(η4-C4Me4)(η5-C5H5)] |
| Authors of publication | Chadha, Preeti; Dutton, Jason L.; Sgro, Michael J.; Ragogna, Paul J. |
| Journal of publication | Organometallics |
| Year of publication | 2007 |
| Journal volume | 26 |
| Journal issue | 25 |
| Pages of publication | 6063 |
| a | 8.0983 ± 0.0011 Å |
| b | 8.9558 ± 0.0012 Å |
| c | 20.885 ± 0.003 Å |
| α | 87.9573 ± 0.0019° |
| β | 86.5522 ± 0.0018° |
| γ | 77.6112 ± 0.0017° |
| Cell volume | 1476.4 ± 0.4 Å3 |
| Cell temperature | 193 ± 2 K |
| Ambient diffraction temperature | 193 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0396 |
| Residual factor for significantly intense reflections | 0.036 |
| Weighted residual factors for significantly intense reflections | 0.1167 |
| Weighted residual factors for all reflections included in the refinement | 0.119 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.164 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178629 (current) | 2016-03-21 | cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/40. |
4074071.cif |
| 120075 | 2014-07-11 | Adding DOIs to range 4/07 structures. | 4074071.cif |
| 47256 | 2012-03-23 | cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories. |
4074071.cif |
| 46717 | 2012-03-21 | ../uploads/cif-deposit/cod/cif Adding structures of 4074070, 4074071 via cif-deposit CGI script. |
4074071.cif |
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Users of the data should acknowledge the original authors of the
structural data.