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Information card for entry 4074104
Preview
| Coordinates | 4074104.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C73 H61 Cl13 N8 O5 Ru2 |
|---|---|
| Calculated formula | C72.532 H60.064 Cl13 N8 O5.258 Ru2 |
| Title of publication | Negishi Couplingî—¸Expedient Formation of Biphenyls on the Periphery of Inorganic/Organometallic Diruthenium Species |
| Authors of publication | Zhang, Lei; Huang, Zhihong; Chen, Wei-Zhong; Negishi, Ei-ichi; Fanwick, Phillip E.; Updegraff, James B.; Protasiewicz, John D.; Ren, Tong |
| Journal of publication | Organometallics |
| Year of publication | 2007 |
| Journal volume | 26 |
| Journal issue | 26 |
| Pages of publication | 6526 |
| a | 16.1963 ± 0.0002 Å |
| b | 18.3611 ± 0.0003 Å |
| c | 27.7087 ± 0.0004 Å |
| α | 88.5192 ± 0.0006° |
| β | 75.1286 ± 0.0005° |
| γ | 77.435 ± 0.0008° |
| Cell volume | 7769.4 ± 0.2 Å3 |
| Cell temperature | 150 K |
| Ambient diffraction temperature | 150 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.084 |
| Residual factor for significantly intense reflections | 0.058 |
| Weighted residual factors for significantly intense reflections | 0.141 |
| Weighted residual factors for all reflections included in the refinement | 0.155 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.023 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MO-Kα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 178630 (current) | 2016-03-21 | cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/41. |
4074104.cif |
| 120075 | 2014-07-11 | Adding DOIs to range 4/07 structures. | 4074104.cif |
| 47256 | 2012-03-23 | cif/4/ Distributing the new range 4 CIFs into their appropriate prefixed subdirectories. |
4074104.cif |
| 46744 | 2012-03-21 | ../uploads/cif-deposit/cod/cif Adding structures of 4074104, 4074105 via cif-deposit CGI script. |
4074104.cif |
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Users of the data should acknowledge the original authors of the
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