Crystallography Open Database

Information card for entry 4074661

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Structure parameters

Formula	C24 H30 B Ge Li
Calculated formula	C24 H30 B Ge Li
Title of publication	Preparation, Structural Characterization, and Photochemical Reactions of Silyl- and Germylborates
Authors of publication	Nanjo, Masato; Matsudo, Kazuhiko; Kurihara, Mari; Nakamura, Sayaka; Sakaguchi, Yoshio; Hayashi, Hisaharu; Mochida, Kunio
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	4
Pages of publication	832
a	12.164 ± 0.0012 Å
b	11.328 ± 0.0005 Å
c	16.122 ± 0.0014 Å
α	90°
β	100.114 ± 0.004°
γ	90°
Cell volume	2187 ± 0.3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0441
Residual factor for significantly intense reflections	0.0362
Weighted residual factors for significantly intense reflections	0.1069
Weighted residual factors for all reflections included in the refinement	0.1153
Goodness-of-fit parameter for all reflections included in the refinement	0.945
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
301830 (current)	2025-08-20	Add cross-references to PubChem compounds in COD range 4/07/ Each referenced PubChem compound corresponds to the full crystal structure.	4074661.cif
178635	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/46.	4074661.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4074661.cif
107967	2014-03-25	cif/4 Changing the entity to the proper non-English character for many entries in subdir 4	4074661.cif
48636	2012-03-27	../uploads/cif-deposit/cod/cif Adding structures of 4074661 via cif-deposit CGI script.	4074661.cif