Crystallography Open Database

Information card for entry 4074662

Preview

Coordinates	4074662.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H33 B Ge Li O3
Calculated formula	C27 H41 B Ge Li O3
Title of publication	Preparation, Structural Characterization, and Photochemical Reactions of Silyl- and Germylborates
Authors of publication	Nanjo, Masato; Matsudo, Kazuhiko; Kurihara, Mari; Nakamura, Sayaka; Sakaguchi, Yoshio; Hayashi, Hisaharu; Mochida, Kunio
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	4
Pages of publication	832
a	11.192 ± 0.0009 Å
b	11.083 ± 0.0006 Å
c	11.537 ± 0.001 Å
α	84.692 ± 0.005°
β	84.914 ± 0.004°
γ	86.971 ± 0.005°
Cell volume	1417.87 ± 0.18 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.039
Residual factor for significantly intense reflections	0.0367
Weighted residual factors for significantly intense reflections	0.1207
Weighted residual factors for all reflections included in the refinement	0.1238
Goodness-of-fit parameter for all reflections included in the refinement	1.125
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178635 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/46.	4074662.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4074662.cif
107967	2014-03-25	cif/4 Changing the entity to the proper non-English character for many entries in subdir 4	4074662.cif
48637	2012-03-27	../uploads/cif-deposit/cod/cif Adding structures of 4074662 via cif-deposit CGI script.	4074662.cif