Crystallography Open Database

Information card for entry 4075085

Preview

Coordinates	4075085.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C19 H31 B Ge N2 Si2
Calculated formula	C19 H31 B Ge N2 Si2
SMILES	[GeH]1([BH3])[n]2ccccc2C([Si](C)(C)C)=C(N1[Si](C)(C)C)c1ccccc1
Title of publication	Reactivity of Pyridyl-1-azaallyl Germanium(II) Chloride: Synthesis of Novel Lithium Germinate [{(PhC⋮C)3Ge}3GeLi(Et2O)3] and Ge(II)−M(I) (M = Cu and Au) Adducts
Authors of publication	Leung, Wing-Por; So, Cheuk-Wai; Chong, Kim-Hung; Kan, Kwok-Wai; Chan, Hoi-Shan; Mak, Thomas C. W.
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	11
Pages of publication	2851
a	18.195 ± 0.004 Å
b	11.688 ± 0.002 Å
c	11.192 ± 0.002 Å
α	90°
β	99.29 ± 0.03°
γ	90°
Cell volume	2348.9 ± 0.8 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0585
Residual factor for significantly intense reflections	0.0542
Weighted residual factors for significantly intense reflections	0.149
Weighted residual factors for all reflections included in the refinement	0.1591
Goodness-of-fit parameter for all reflections included in the refinement	1.165
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178639 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/50.	4075085.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4075085.cif
49056	2012-03-27	../uploads/cif-deposit/cod/cif Adding structures of 4075085 via cif-deposit CGI script.	4075085.cif