Crystallography Open Database

Information card for entry 4075086

Preview

Coordinates	4075086.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H32 Ge N2 Si2
Calculated formula	C27 H32 Ge N2 Si2
SMILES	[Ge]1([n]2ccccc2C([Si](C)(C)C)=C(N1[Si](C)(C)C)c1ccccc1)C#Cc1ccccc1
Title of publication	Reactivity of Pyridyl-1-azaallyl Germanium(II) Chloride: Synthesis of Novel Lithium Germinate [{(PhC⋮C)3Ge}3GeLi(Et2O)3] and Ge(II)−M(I) (M = Cu and Au) Adducts
Authors of publication	Leung, Wing-Por; So, Cheuk-Wai; Chong, Kim-Hung; Kan, Kwok-Wai; Chan, Hoi-Shan; Mak, Thomas C. W.
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	11
Pages of publication	2851
a	8.3622 ± 0.0017 Å
b	11.227 ± 0.002 Å
c	16.899 ± 0.003 Å
α	107.28 ± 0.03°
β	90.39 ± 0.03°
γ	100.47 ± 0.03°
Cell volume	1486.6 ± 0.6 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0571
Residual factor for significantly intense reflections	0.0524
Weighted residual factors for significantly intense reflections	0.1413
Weighted residual factors for all reflections included in the refinement	0.1486
Goodness-of-fit parameter for all reflections included in the refinement	1.062
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178639 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/50.	4075086.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4075086.cif
49057	2012-03-27	../uploads/cif-deposit/cod/cif Adding structures of 4075086 via cif-deposit CGI script.	4075086.cif