Crystallography Open Database

Information card for entry 4077668

Preview

Coordinates	4077668.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C47 H82 B20 Li O6 Yb
Calculated formula	C47 H82 B20 Li O6 Yb
Title of publication	Carbon versus Silicon Bridges. Synthesis of a New Versatile Ligand and Its Applications in Organolanthanide Chemistry
Authors of publication	Wang, Shaowu; Yang, Qingchuan; Mak, Thomas C. W.; Xie, Zuowei
Journal of publication	Organometallics
Year of publication	2000
Journal volume	19
Journal issue	3
Pages of publication	334
a	12.716 ± 0.003 Å
b	21.471 ± 0.004 Å
c	22.011 ± 0.004 Å
α	90°
β	90°
γ	90°
Cell volume	6010 ± 2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0628
Residual factor for significantly intense reflections	0.0574
Weighted residual factors for significantly intense reflections	0.1477
Weighted residual factors for all reflections included in the refinement	0.1523
Goodness-of-fit parameter for all reflections included in the refinement	1.059
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178665 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/76.	4077668.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4077668.cif
54660	2012-04-28	cif/ Adding structures of 4077665, 4077666, 4077667, 4077668, 4077669, 4077670, 4077671 via cif-deposit CGI script.	4077668.cif