Crystallography Open Database

Information card for entry 4077669

Preview

Coordinates	4077669.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H64 B20 Li O4 Yb
Calculated formula	C36 H62 B20 Li O4 Yb
Title of publication	Carbon versus Silicon Bridges. Synthesis of a New Versatile Ligand and Its Applications in Organolanthanide Chemistry
Authors of publication	Wang, Shaowu; Yang, Qingchuan; Mak, Thomas C. W.; Xie, Zuowei
Journal of publication	Organometallics
Year of publication	2000
Journal volume	19
Journal issue	3
Pages of publication	334
a	11.551 ± 0.003 Å
b	12.899 ± 0.003 Å
c	16.805 ± 0.004 Å
α	79.912 ± 0.008°
β	76.46 ± 0.019°
γ	83.453 ± 0.017°
Cell volume	2389.7 ± 1 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0994
Residual factor for significantly intense reflections	0.0956
Weighted residual factors for significantly intense reflections	0.245
Weighted residual factors for all reflections included in the refinement	0.2477
Goodness-of-fit parameter for all reflections included in the refinement	1.171
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178665 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/76.	4077669.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4077669.cif
54660	2012-04-28	cif/ Adding structures of 4077665, 4077666, 4077667, 4077668, 4077669, 4077670, 4077671 via cif-deposit CGI script.	4077669.cif