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Information card for entry 4078489
Preview
Coordinates | 4078489.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C30.92 H46.76 B2 I0.08 N12 U |
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Calculated formula | C30.921 H46.763 B2 I0.079 N12 U |
Title of publication | Use of Alkylsodium Reagents for the Synthesis of Trivalent Uranium Alkyl Complexes |
Authors of publication | Matson, Ellen M.; Forrest, William P.; Fanwick, Phillip E.; Bart, Suzanne C. |
Journal of publication | Organometallics |
Year of publication | 2012 |
Journal volume | 31 |
Journal issue | 12 |
Pages of publication | 4467 |
a | 10.2751 ± 0.0007 Å |
b | 10.7169 ± 0.0009 Å |
c | 18.3052 ± 0.0013 Å |
α | 96.786 ± 0.007° |
β | 100.517 ± 0.006° |
γ | 115.091 ± 0.006° |
Cell volume | 1751 ± 0.3 Å3 |
Cell temperature | 150 ± 0.2 K |
Ambient diffraction temperature | 150 ± 0.2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.064 |
Residual factor for significantly intense reflections | 0.06 |
Weighted residual factors for significantly intense reflections | 0.163 |
Weighted residual factors for all reflections included in the refinement | 0.167 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.105 |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CU-Kα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
288505 (current) | 2023-12-22 | Corrected misspelt data names in multiple entries using the 'cif_correct_tags' program and a data name replacement file from cod-tools revision 9880. This change affected only the misspelt variants of the '_iucr_refine_instructions_details' data name. |
4078489.cif |
176467 | 2016-02-16 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4. |
4078489.cif |
91935 | 2013-12-29 | cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs. |
4078489.cif |
62397 | 2012-07-07 | cif/ Adding structures of 4078489 via cif-deposit CGI script. |
4078489.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
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.
Users of the data should acknowledge the original authors of the
structural data.