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Information card for entry 4078490
Preview
| Coordinates | 4078490.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C37 H62 B2 N12 Si U |
|---|---|
| Calculated formula | C37 H62 B2 N12 Si U |
| Title of publication | Use of Alkylsodium Reagents for the Synthesis of Trivalent Uranium Alkyl Complexes |
| Authors of publication | Matson, Ellen M.; Forrest, William P.; Fanwick, Phillip E.; Bart, Suzanne C. |
| Journal of publication | Organometallics |
| Year of publication | 2012 |
| Journal volume | 31 |
| Journal issue | 12 |
| Pages of publication | 4467 |
| a | 12.6822 ± 0.0008 Å |
| b | 13.1029 ± 0.001 Å |
| c | 14.4609 ± 0.001 Å |
| α | 78.889 ± 0.005° |
| β | 66.013 ± 0.005° |
| γ | 84.836 ± 0.004° |
| Cell volume | 2154.2 ± 0.3 Å3 |
| Cell temperature | 150 ± 0.2 K |
| Ambient diffraction temperature | 150 ± 0.2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.066 |
| Residual factor for significantly intense reflections | 0.055 |
| Weighted residual factors for significantly intense reflections | 0.129 |
| Weighted residual factors for all reflections included in the refinement | 0.138 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.063 |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CU-Kα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 288505 (current) | 2023-12-22 | Corrected misspelt data names in multiple entries using the 'cif_correct_tags' program and a data name replacement file from cod-tools revision 9880. This change affected only the misspelt variants of the '_iucr_refine_instructions_details' data name. |
4078490.cif |
| 176467 | 2016-02-16 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4. |
4078490.cif |
| 91935 | 2013-12-29 | cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs. |
4078490.cif |
| 62398 | 2012-07-07 | cif/ Adding structures of 4078490 via cif-deposit CGI script. |
4078490.cif |
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Users of the data should acknowledge the original authors of the
structural data.