Crystallography Open Database

Information card for entry 4080091

Preview

Coordinates	4080091.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H71 Ge O2 P
Calculated formula	C48 H71 Ge O2 P
Title of publication	Versatile Reactivity of Phosphagermaallene Tip(t-Bu)Ge═C═PMes* with α-Ethylenic Esters
Authors of publication	Ghereg, Dumitru; Ouhsaine, Fatima; Escudié, Jean; Labat, Stéphane; André, Erwan; Miqueu, Karinne; Sotiropoulos, Jean-Marc; Gornitzka, Heinz; Saffon, Nathalie
Journal of publication	Organometallics
Year of publication	2013
Journal volume	32
Journal issue	4
Pages of publication	1085
a	18.7194 ± 0.0014 Å
b	9.3375 ± 0.0007 Å
c	26.805 ± 0.002 Å
α	90°
β	102.426 ± 0.001°
γ	90°
Cell volume	4575.6 ± 0.6 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0485
Residual factor for significantly intense reflections	0.0346
Weighted residual factors for significantly intense reflections	0.0839
Weighted residual factors for all reflections included in the refinement	0.0914
Goodness-of-fit parameter for all reflections included in the refinement	1.031
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178689 (current)	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/00.	4080091.cif
75527	2013-03-10	cif/ Adding structures of 4080091, 4080092, 4080093 via cif-deposit CGI script.	4080091.cif