Crystallography Open Database

Information card for entry 4080092

Preview

Coordinates	4080092.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C43 H67 Ge O4 P
Calculated formula	C43 H67 Ge O4 P
Title of publication	Versatile Reactivity of Phosphagermaallene Tip(t-Bu)Ge═C═PMes* with α-Ethylenic Esters
Authors of publication	Ghereg, Dumitru; Ouhsaine, Fatima; Escudié, Jean; Labat, Stéphane; André, Erwan; Miqueu, Karinne; Sotiropoulos, Jean-Marc; Gornitzka, Heinz; Saffon, Nathalie
Journal of publication	Organometallics
Year of publication	2013
Journal volume	32
Journal issue	4
Pages of publication	1085
a	10.4119 ± 0.0012 Å
b	22.586 ± 0.002 Å
c	18.438 ± 0.002 Å
α	90°
β	100.725 ± 0.002°
γ	90°
Cell volume	4260.2 ± 0.8 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1496
Residual factor for significantly intense reflections	0.0592
Weighted residual factors for significantly intense reflections	0.1096
Weighted residual factors for all reflections included in the refinement	0.1411
Goodness-of-fit parameter for all reflections included in the refinement	0.979
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178689 (current)	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/00.	4080092.cif
75527	2013-03-10	cif/ Adding structures of 4080091, 4080092, 4080093 via cif-deposit CGI script.	4080092.cif