Crystallography Open Database

Information card for entry 4083428

Preview

Coordinates	4083428.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H32 N2 Pt Si
Calculated formula	C27 H32 N2 Pt Si
SMILES	[PtH2]1([Si](CC)(CC)CC)[n]2c(c3n1c(c1ccccc1)cc3c1ccccc1)cccc2
Title of publication	Five-Coordinate Dihydridosilyl Platinum(IV) Complexes Supported by a Chelating Monoanionic Nitrogen-Based Ligand
Authors of publication	McBee, Jennifer L.; Tilley, T. Don
Journal of publication	Organometallics
Year of publication	2009
Journal volume	28
Journal issue	13
Pages of publication	3947 - 3952
a	41.674 ± 0.008 Å
b	9.7404 ± 0.0018 Å
c	24.917 ± 0.005 Å
α	90°
β	104.912 ± 0.003°
γ	90°
Cell volume	9774 ± 3 Å³
Cell temperature	146 ± 2 K
Ambient diffraction temperature	146 ± 2 K
Number of distinct elements	5
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.0834
Residual factor for significantly intense reflections	0.0516
Weighted residual factors for significantly intense reflections	0.0874
Weighted residual factors for all reflections included in the refinement	0.1013
Goodness-of-fit parameter for all reflections included in the refinement	1.018
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Duplicate of	4069551
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
209982 (current)	2018-08-20	cif/4/ Updating bibliography in entries 4069551, 4083428. Marking entry 4083428 as a duplicate of entry 4069551.	4083428.cif
178723	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/34.	4083428.cif
170212	2015-11-09	cif/4: Fixing some Z values and formulae.	4083428.cif
114878	2014-05-29	cif/ Adding structures of 4083428 via cif-deposit CGI script.	4083428.cif