Crystallography Open Database

Information card for entry 4085346

Preview

Coordinates	4085346.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H42 N2 O2 Sn
Calculated formula	C32 H42 N2 O2 Sn
Title of publication	Oxidative Additions of Homoleptic Tin(II) Amidinate
Authors of publication	Chlupatý, Tomáš; Růžičková, Zdeňka; Horáček, Michal; Alonso, Mercedes; De Proft, Frank; Kampová, Hana; Brus, Jiří; Růžička, Aleš
Journal of publication	Organometallics
Year of publication	2015
Journal volume	34
Journal issue	3
Pages of publication	606
a	8.455 ± 0.0004 Å
b	11.1981 ± 0.0005 Å
c	15.7039 ± 0.0011 Å
α	86.51 ± 0.006°
β	77.977 ± 0.005°
γ	87.67 ± 0.006°
Cell volume	1450.94 ± 0.14 Å³
Cell temperature	150 ± 1 K
Ambient diffraction temperature	150 ± 1 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0281
Residual factor for significantly intense reflections	0.0232
Weighted residual factors for significantly intense reflections	0.0528
Weighted residual factors for all reflections included in the refinement	0.056
Goodness-of-fit parameter for all reflections included in the refinement	1.082
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178742 (current)	2016-03-21	cif/4/08/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/08/53.	4085346.cif
132972	2015-03-04	cif/ Updating files of 4085339, 4085340, 4085341, 4085342, 4085343, 4085344, 4085345, 4085346 Original log message: Adding full bibliography for 4085339--4085346.cif.	4085346.cif
130840	2015-02-04	cif/ Adding structures of 4085339, 4085340, 4085341, 4085342, 4085343, 4085344, 4085345, 4085346 via cif-deposit CGI script.	4085346.cif